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2 article(s) from Mahgoub, Aya

Gold(I) N-heterocyclic carbene precursors for focused electron beam-induced deposition

Cristiano Glessi,
Aya Mahgoub,
Cornelis W. Hagen and
Mats Tilset

Beilstein J. Nanotechnol. 2021, 12, 257–269, doi:10.3762/bjnano.12.21

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Figure 1: Overview of previously reported FEBID gold precursors, Au(acac)Me₂ [10,20-22], Au(tfac)Me₂ [21,23-25], Au(hfac)Me₂ [19], Au...

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Figure 2: Substrate heater and precursor supply system of the deposition setup. Only the conical hole in the ...

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Figure 3: The selected Au(NHC)X complexes studied and their molecular formulae.

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Scheme 1: Synthesis routes for 1–7.

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Figure 4: SEM images, tilted by 50°, of 250 × 250 nm² square deposits made using a beam energy and current of...

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Figure 5: Possible fragmentations of (N,Et)AuCl (6), with the loss of Cl and a volatile fragment 6b, and the ...

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Figure 6: Typical SEM images, tilted by 50°, of pillar arrays deposited from all precursors. (a) 1 (Cl,Me)AuC...

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Figure 7: Calculated volume of pillars grown using a 5 kV, 40 pA beam, as a function of the electron dose giv...

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Published 17 Mar 2021

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Electron beam-induced deposition of platinum from Pt(CO)₂Cl₂ and Pt(CO)₂Br₂

Aya Mahgoub,
Hang Lu,
Rachel M. Thorman,
Konstantin Preradovic,
Titel Jurca,
Lisa McElwee-White,
Howard Fairbrother and
Cornelis W. Hagen

Beilstein J. Nanotechnol. 2020, 11, 1789–1800, doi:10.3762/bjnano.11.161

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Figure 1: Thermogravimetric analysis (TGA) and 1st derivative DTG of (a) Pt(CO)₂Cl₂ and (b) Pt(CO)₂Br₂.

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Figure 2: Isothermal TGA traces plotted as a function of temperature and time for (a,b) Pt(CO)₂Cl₂ and (c,d) ...

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Figure 3: Chamber pressure after opening and closing the GIS valve containing a) Pt(CO)₂Cl₂ and b) MeCpPtMe₃.

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Figure 4: Pillars deposited at 38 pA. a) 35° tilt image of pillars deposited from top to bottom and from left...

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Figure 5: Pillar height a) and volume b) as functions of the electron dose (total number of incident electron...

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Figure 6: Comparison of pillars grown in experiment 2 from all three precursors a) and d) MeCpPtMe₃, b) and e...

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Figure 7: Pillar height a) and volume b) as functions of the number of electrons deposited at 38 pA from MeCp...

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Published 27 Nov 2020

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Gold(I) N-heterocyclic carbene precursors for focused electron beam-induced deposition

Electron beam-induced deposition of platinum from Pt(CO)2Cl2 and Pt(CO)2Br2

Electron beam-induced deposition of platinum from Pt(CO)₂Cl₂ and Pt(CO)₂Br₂